A process for the preparation of improved friction dust useful as friction modifier in brake/clutch facings which comprises preparing a slurry of phosphorylated cashewnut shell liquid prepolymer and a cross-linking agent in an organic solvent such as herein described, mixing the said slurry in a conventional mixer of a period ranging 20 to 30 minutes, pulverizing the resultant dust, sieving and thermohardening the obtained dust at a temperature in the range of 80 - 13°C for a period of 20 to 30 minutes to get the desired improved friction dust.
The present invention provides a process for the preparation of improved friction dust useful as friction modifier in brake / clutch facings. As the friction dust prepared from phosphorylated cashew nut shell liquid prepolymer by the process of the present invention possesses properties superior to that of the conventional
CNSL- formaldehyde resin in terms of improved resistance to flame, high temperature stability, lower fade value, better durability etc., it can be used as a friction modifier in brake linings substituting the existing brands that are known to give rise to serious problems. So the industries to which the invention can apply are brake lining and clutch facing industries.
Friction dust is generally prepared from CNSL- formaldehyde resin or from the residue known as residol obtained after distillation of cardanol from CNSL.
The CNSL resin is then cross-linked with hexamine or paraformaldehyde and cured, further thermohardened and ground to a coarse dust.
The residol route is mostly preferred by the industry as it is more cost effective. The preparation, properties and specification of friction dust are trade secrets and published literature are rare. Addition of friction dust is expected to modify frictional and wear properties of the brake linings.
An increase of 30-40 % in wear improvement is expected. It also helps in reducing the fade value and lowering the noise level thereby giving the brake lining enhanced life and a quieter braking action. However, the conventional material was found to give serious problems: The friction dust prepared through this route is suspected to catch fire during shipments and hence its export market has eroded greatly. So it was thought necessary to develop a process to prepare friction dust having improved thermal stability and better resistance to flammability.
The main object of the invention is to provide a process for the preparation of friction dust useful as a friction modifier in brake / clutch linings, Another object of the present invention is to provide a process for the preparation of friction dust from phosphorylated cashewnut shell liquid prepolymer having improved resistance to flame and better high temperature stability and better fade and other friction modifying ptoperties than the conventional friction products.
Source: http://www.allindianpatents.com/patents/242267-a-process-for-the-preparation-of-improved-friction-dust-useful-as-friction-modifier-in-brake-clutch-facings